Synthesis and Crystal Structure of 1-(2-Hydroxy-4-methoxyphenyl)-2-phenyl-1-ethanone
نویسندگان
چکیده
منابع مشابه
Crystal structure of (-)-(1'R)-1-(2'-hydroxy-1'-phenyl-ethyl)-1H-pyridin-2-one.
wide interest because the 1H-pyridin-2-ones obtained in this process are versatile synthetic building blocks in the synthesis of alkaloids.1–5 The title compound, (–)-(1′R)-1-(2′-hydroxy-1′-phenyl-ethyl)1H-pyridin-2-one II, was prepared by stirring a solution of pyridinium salt, I (4.0 mmol), in water (25 ml) and cooled to 5 ̊C (Scheme 1). A solution of K3Fe(CN)6 (11 eq.) in water (30 ml) was ad...
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A new 2-[(4-substituted-phenyl-3-chloroazetidin-2-one)-5-(2'-methylamino 4-phenyl-1', 3'-thiazolyl-]-1, 3, 4-thiadiazoles, 5(a-n) were synthesized from 2-substituted-benzylideneamino-5-[2'-methylamino-4'-phenyl-1',3'-thiazolyl]-1,3, 4-thiadiazole, 4(a-n) using 2-amino-4phenyl-1, 3-thiazole as a starting material. The synthesised compounds have been screened in vitro for their antimicrobial acti...
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The title compound, C(29)H(20)ClNOS, is a 1-substituted-3-phenyl-isoquinoline that crystallizes with four independent mol-ecules in the asymmtric unit. The four mol-ecules have similar C-S-C angles. The most noteworthy differences between the mol-ecules relate to the inclination of the 3-phenyl subsituent with respect to the isoquinoline fused-ring [dihedral angles of 21.2 (1), 25.6 (2), 34.3 (...
متن کاملCrystal structure of 2-meth-oxy-2-[(4-meth-oxy-phen-yl)sulfan-yl]-1-phenyl-ethanone.
In the title β-thio-carbonyl compound, C16H16O3S, the adjacent meth-oxy and carbonyl O atoms are synperiplanar [the O-C-C-O torsion angle is 19.8 (4)°] and are separated by 2.582 (3) Å. The dihedral angle between the rings is 40.11 (16)°, and the meth-oxy group is coplanar with the benzene ring to which it is connected [the C-C-O-C torsion angle is 179.1 (3)°]. The most notable feature of the c...
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ژورنال
عنوان ژورنال: Analytical Sciences: X-ray Structure Analysis Online
سال: 2007
ISSN: 1348-2238
DOI: 10.2116/analscix.23.x153